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Information card for entry 4327299
Preview
Coordinates | 4327299.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C4 H80 Mo6 N10 O55 P8 |
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Calculated formula | C4 H8 Mo6 O58.5 P8 |
Title of publication | Synthesis and Characterization of Octa- and Hexanuclear Polyoxomolybdate Wheels: Role of the Inorganic Template and of the Counterion |
Authors of publication | Anne Dolbecq; Laurent Lisnard; Pierre Mialane; Jérôme Marrot; Marc Bénard; Marie-Madeleine Rohmer; Francis Sécheresse |
Journal of publication | Inorganic Chemistry |
Year of publication | 2006 |
Journal volume | 45 |
Pages of publication | 5898 - 5910 |
a | 13.4897 ± 0.0002 Å |
b | 13.7119 ± 0.0002 Å |
c | 17.9603 ± 0.0001 Å |
α | 73.936 ± 0.001° |
β | 77.086 ± 0.001° |
γ | 64.9 ± 0.001° |
Cell volume | 2869.36 ± 0.07 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.114 |
Residual factor for significantly intense reflections | 0.0768 |
Weighted residual factors for significantly intense reflections | 0.1983 |
Weighted residual factors for all reflections included in the refinement | 0.214 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.154 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
179375 (current) | 2016-03-23 | cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/72. |
4327299.cif |
120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4327299.cif |
61015 | 2012-06-20 | cif/ Adding structures of 4327299 via cif-deposit CGI script. |
4327299.cif |
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Users of the data should acknowledge the original authors of the
structural data.