Crystallography Open Database

Information card for entry 4327305

Preview

Coordinates	4327305.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H30 Gd N11 Ni2 O15
Calculated formula	C30 H20 Gd N11 Ni2 O15
Title of publication	Novel Heterometallic 3d-4f Metal-Azido Complex of Mixed Ligands with Unprecedented Structure Type: Synthesis, Structure, and Magnetic Properties
Authors of publication	Fu-Chen Liu; Yong-Fei Zeng; Jiao Jiao; Jian-Rong Li; Xian-He Bu; Joan Ribas; Stuart R. Batten
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Pages of publication	6129 - 6131
a	8.1859 ± 0.0009 Å
b	26.853 ± 0.003 Å
c	16.8859 ± 0.0018 Å
α	90°
β	95.351 ± 0.002°
γ	90°
Cell volume	3695.6 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0315
Residual factor for significantly intense reflections	0.0283
Weighted residual factors for significantly intense reflections	0.0789
Weighted residual factors for all reflections included in the refinement	0.0807
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179376 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/73.	4327305.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327305.cif
61021	2012-06-20	cif/ Adding structures of 4327305 via cif-deposit CGI script.	4327305.cif