Crystallography Open Database

Information card for entry 4327353

Preview

Coordinates	4327353.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C79 H76 Cl Cu3 F6 O2 P8 S2
Calculated formula	C79 H76 Cl Cu3 F6 O2 P8 S2
Title of publication	Versatility of Dithiophosphates in the Syntheses of Copper(I) Complexes with Bis(diphenylphosphino)alkanes: Abstraction of Chloride from Dichloromethane
Authors of publication	Ben-Jie Liaw; Tarlok S. Lobana; Ya-Wen Lin; Ju-Chun Wang; C. W. Liu
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	9921 - 9929
a	11.2129 ± 0.001 Å
b	14.1419 ± 0.0012 Å
c	25.91 ± 0.002 Å
α	95.328 ± 0.002°
β	99.594 ± 0.002°
γ	102.581 ± 0.002°
Cell volume	3918.1 ± 0.6 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0466
Residual factor for significantly intense reflections	0.0391
Weighted residual factors for significantly intense reflections	0.0993
Weighted residual factors for all reflections included in the refinement	0.1053
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179376 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/73.	4327353.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327353.cif
61117	2012-06-21	cif/ Adding structures of 4327353 via cif-deposit CGI script.	4327353.cif