Crystallography Open Database

Information card for entry 4327356

Preview

Coordinates	4327356.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H84 Cu4 O8 P8 S8
Calculated formula	C66 H64 Cu4 O8 P8 S8
Title of publication	Versatility of Dithiophosphates in the Syntheses of Copper(I) Complexes with Bis(diphenylphosphino)alkanes: Abstraction of Chloride from Dichloromethane
Authors of publication	Ben-Jie Liaw; Tarlok S. Lobana; Ya-Wen Lin; Ju-Chun Wang; C. W. Liu
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	9921 - 9929
a	13.4731 ± 0.0006 Å
b	23.888 ± 0.001 Å
c	24.6483 ± 0.001 Å
α	90°
β	95.986 ± 0.001°
γ	90°
Cell volume	7889.7 ± 0.6 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0594
Residual factor for significantly intense reflections	0.0348
Weighted residual factors for significantly intense reflections	0.0859
Weighted residual factors for all reflections included in the refinement	0.0951
Goodness-of-fit parameter for all reflections included in the refinement	0.926
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179376 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/73.	4327356.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327356.cif
61120	2012-06-21	cif/ Adding structures of 4327356 via cif-deposit CGI script.	4327356.cif