Crystallography Open Database

Information card for entry 4327359

Preview

Coordinates	4327359.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C61 H68 Cl2 Cu2 O4 P6 S4
Calculated formula	C61 H68 Cl2 Cu2 O4 P6 S4
Title of publication	Versatility of Dithiophosphates in the Syntheses of Copper(I) Complexes with Bis(diphenylphosphino)alkanes: Abstraction of Chloride from Dichloromethane
Authors of publication	Ben-Jie Liaw; Tarlok S. Lobana; Ya-Wen Lin; Ju-Chun Wang; C. W. Liu
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	9921 - 9929
a	11.752 ± 0.002 Å
b	13.127 ± 0.002 Å
c	13.268 ± 0.003 Å
α	61.126 ± 0.015°
β	76.858 ± 0.008°
γ	68.48 ± 0.013°
Cell volume	1664.3 ± 0.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0942
Residual factor for significantly intense reflections	0.0663
Weighted residual factors for significantly intense reflections	0.164
Weighted residual factors for all reflections included in the refinement	0.1862
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179376 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/73.	4327359.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327359.cif
61123	2012-06-21	cif/ Adding structures of 4327359 via cif-deposit CGI script.	4327359.cif