Crystallography Open Database

Information card for entry 4327362

Preview

Coordinates	4327362.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6 H6 K3 O15 V
Calculated formula	C6 H6 K3 O15 V
Title of publication	Synthesis, Structure, and Magnetic Ordering of Layered (2-D) V-Based Tris(oxalato)metalates
Authors of publication	Kil Sik Min; Arnold L. Rhinegold; Joel S. Miller
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	8433 - 8441
a	7.7303 ± 0.0006 Å
b	19.9435 ± 0.0016 Å
c	10.2616 ± 0.0008 Å
α	90°
β	107.671 ± 0.001°
γ	90°
Cell volume	1507.4 ± 0.2 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0332
Residual factor for significantly intense reflections	0.0292
Weighted residual factors for significantly intense reflections	0.0772
Weighted residual factors for all reflections included in the refinement	0.0805
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179376 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/73.	4327362.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327362.cif
61126	2012-06-21	cif/ Adding structures of 4327362 via cif-deposit CGI script.	4327362.cif