Crystallography Open Database

Information card for entry 4327476

Preview

Coordinates	4327476.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(Rb-18C6)8(Ge9=Ge9=Ge9=Ge9).2en (1)
Formula	C100 H208 Ge36 N4 O48 Rb8
Calculated formula	C100 H208.04 Ge36 N4 O48 Rb8
Title of publication	[Ge9Ge9Ge9Ge9]8-: A Linear Tetramer of Nine-Atom Germanium Clusters, a Nanorod
Authors of publication	Angel Ugrinov; Slavi C. Sevov
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	5789 - 5791
a	15.1198 ± 0.001 Å
b	16.2502 ± 0.0011 Å
c	18.7173 ± 0.0012 Å
α	83.304 ± 0.001°
β	83.012 ± 0.001°
γ	78.003 ± 0.001°
Cell volume	4445.2 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0975
Residual factor for significantly intense reflections	0.0576
Weighted residual factors for significantly intense reflections	0.1315
Weighted residual factors for all reflections included in the refinement	0.1505
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179377 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/74.	4327476.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327476.cif
61279	2012-06-26	cif/4 Fixing wrong year of publication of several entries (there was a mistake when these files were deposited)	4327476.cif
61247	2012-06-25	cif/ Adding structures of 4327476 via cif-deposit CGI script.	4327476.cif