Crystallography Open Database

Information card for entry 4327689

Preview

Coordinates	4327689.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H37 N2 P Pt S W2
Calculated formula	C240 H296 N16 P8 Pt8 S64 W16
Title of publication	Syntheses and Structures of Mixed-Metal Sulfido Clusters Containing Trimetallic M2M'S4 (M = Mo, W; M' = Pd, Pt) and Tetrametallic Cubane-Type Mo2Pd2S4 Cores
Authors of publication	Tomotake Ikada; Shigeki Kuwata; Yasushi Mizobe; Masanobu Hidai
Journal of publication	Inorganic Chemistry
Year of publication	1998
Journal volume	37
Pages of publication	5793 - 5797
a	13.718 ± 0.003 Å
b	12.795 ± 0.002 Å
c	43.798 ± 0.002 Å
α	90°
β	95.24 ± 0.01°
γ	90°
Cell volume	7655 ± 2 Å³
Cell temperature	23 K
Ambient diffraction temperature	23 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.052
Weighted residual factors for significantly intense reflections	0.038
Goodness-of-fit parameter for significantly intense reflections	2.96
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4327689.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327689.cif
61778	2012-07-05	cif/ Adding structures of 4327689 via cif-deposit CGI script.	4327689.cif