Crystallography Open Database

Information card for entry 4327744

Preview

Coordinates	4327744.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H42 N6 O4 Ru
Calculated formula	C38 H42 N6 O3.99 Ru
Title of publication	Synthesis, Reactivity Studies, Structural Aspects, and Solution Behavior of Half Sandwich Ruthenium(II) N,N',N"-Triarylguanidinate Complexes
Authors of publication	Taruna Singh; Ram Kishan; Munirathinam Nethaji; Natesan Thirupathi
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	157 - 169
a	10.277 ± 0.005 Å
b	11.06 ± 0.005 Å
c	16.638 ± 0.005 Å
α	70.932 ± 0.005°
β	77.569 ± 0.005°
γ	82.911 ± 0.005°
Cell volume	1742.6 ± 1.3 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.079
Residual factor for significantly intense reflections	0.0503
Weighted residual factors for significantly intense reflections	0.1391
Weighted residual factors for all reflections included in the refinement	0.168
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179380 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/77.	4327744.cif
76666	2013-03-21	cif/ Adding structures of 4327744 via cif-deposit CGI script.	4327744.cif