Crystallography Open Database

Information card for entry 4327992

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Structure parameters

Formula	C32 H39 Cl Ge N2
Calculated formula	C32 H39 Cl Ge N2
Title of publication	Reactivity of Digermylenes toward Potassium Graphite: Synthesis and Characterization of Germylidenide Anions
Authors of publication	Siew-Peng Chia; Hui-Xian Yeong; Cheuk-Wai So
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	1002 - 1010
a	9.0808 ± 0.0002 Å
b	26.5379 ± 0.0005 Å
c	14.0952 ± 0.0002 Å
α	90°
β	118.933 ± 0.001°
γ	90°
Cell volume	2972.78 ± 0.1 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0952
Residual factor for significantly intense reflections	0.0572
Weighted residual factors for significantly intense reflections	0.1605
Weighted residual factors for all reflections included in the refinement	0.184
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301838 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 4/32/ Each referenced PubChem compound corresponds to the full crystal structure.	4327992.cif
179382	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/79.	4327992.cif
76936	2013-03-22	cif/ Adding structures of 4327992 via cif-deposit CGI script.	4327992.cif