Crystallography Open Database

Information card for entry 4327997

Preview

Coordinates	4327997.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C100 H134.45 Ge4 K4 N4 O12
Calculated formula	C100 H134.446 Ge4 K4 N4 O12
Title of publication	Reactivity of Digermylenes toward Potassium Graphite: Synthesis and Characterization of Germylidenide Anions
Authors of publication	Siew-Peng Chia; Hui-Xian Yeong; Cheuk-Wai So
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	1002 - 1010
a	15.8408 ± 0.0006 Å
b	26.3835 ± 0.0008 Å
c	25.1989 ± 0.0009 Å
α	90°
β	95.867 ± 0.002°
γ	90°
Cell volume	10476.4 ± 0.6 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1615
Residual factor for significantly intense reflections	0.0585
Weighted residual factors for significantly intense reflections	0.1374
Weighted residual factors for all reflections included in the refinement	0.1975
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179382 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/79.	4327997.cif
76941	2013-03-22	cif/ Adding structures of 4327997 via cif-deposit CGI script.	4327997.cif