Crystallography Open Database

Information card for entry 4328373

Preview

Coordinates	4328373.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(Ni(AEPA)2)2((Ni(AEPA)2)V15Sb6O42(H2O))
Formula	C30 H90 N18 Ni3 O50 Sb6 V15
Calculated formula	C30 H90 N18 Ni3 O50 Sb6 V15
Title of publication	Expansion of Antimonato Polyoxovanadates with Transition Metal Complexes: (Co(N3C5H15)2)2[{Co(N3C5H15)2}V15Sb6O42(H2O)].5H2O and (Ni(N3C5H15)2)2[{Ni(N3C5H15)2}V15Sb6O42(H2O)].8H2O
Authors of publication	Elena Antonova; Christian Näther; Paul Kögerler; Wolfgang Bensch
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	2311 - 2317
a	14.5697 ± 0.0013 Å
b	15.8523 ± 0.0016 Å
c	20.2411 ± 0.0018 Å
α	86.702 ± 0.011°
β	84.957 ± 0.011°
γ	76.941 ± 0.011°
Cell volume	4533 ± 0.8 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0491
Residual factor for significantly intense reflections	0.0351
Weighted residual factors for significantly intense reflections	0.0839
Weighted residual factors for all reflections included in the refinement	0.0883
Goodness-of-fit parameter for all reflections included in the refinement	0.949
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179386 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/83.	4328373.cif
77339	2013-03-26	cif/ Adding structures of 4328373 via cif-deposit CGI script.	4328373.cif