Crystallography Open Database

Information card for entry 4328742

Preview

Coordinates	4328742.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C86 H73.5 F1.5 Ge2 Ir O3 P4 Rh
Calculated formula	C86 H73.5 F1.5 Ge2 Ir O3 P4 Rh
Title of publication	Germyl- and Germylene-Bridged Complexes of Rh/Ir and Subsequent Chemistry of a Bridging Germylene Group
Authors of publication	Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	4020 - 4034
a	13.4862 ± 0.0005 Å
b	15.7589 ± 0.0006 Å
c	20.9542 ± 0.0008 Å
α	97.4832 ± 0.0004°
β	104.767 ± 0.0004°
γ	113.785 ± 0.0004°
Cell volume	3801.4 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.02
Residual factor for significantly intense reflections	0.0187
Weighted residual factors for significantly intense reflections	0.0526
Weighted residual factors for all reflections included in the refinement	0.0537
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179390 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/87.	4328742.cif
77740	2013-03-29	cif/ Adding structures of 4328742 via cif-deposit CGI script.	4328742.cif