Crystallography Open Database

Information card for entry 4329212

Preview

Coordinates	4329212.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H58 N2 P2 Si2 Sn
Calculated formula	C32 H58 N2 P2 Si2 Sn
Title of publication	Synthesis and Characterization of N-[2-P(i-Pr)2-4-methylphenyl]2- (PNP) Pincer Tin(IV) and Tin(II) Complexes
Authors of publication	Jens Henning; Hartmut Schubert; Klaus Eichele; Florian Winter; Rainer Pöttgen; Hermann August Mayer; Lars Wesemann
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	5787 - 5794
a	9.6494 ± 0.0003 Å
b	10.6456 ± 0.0003 Å
c	19.0757 ± 0.0005 Å
α	84.389 ± 0.002°
β	85.663 ± 0.002°
γ	71.484 ± 0.002°
Cell volume	1847.12 ± 0.09 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.045
Residual factor for significantly intense reflections	0.0361
Weighted residual factors for significantly intense reflections	0.0779
Weighted residual factors for all reflections included in the refinement	0.0811
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	mokα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
134499 (current)	2015-03-28	cif/ (antanas@echidna.ibt.lt) Fixing misspelled '_atom_site_refinement_flags' tag values (case-sensitive).The issued command: codid2file \| while read file; do cif_fix_values --fix-only-enums --treat-as-set "$file" \| cif_filter -h $file \| sponge $file; done In some cases, tag values did not change, but the tags were reorganized by the 'cif_filter' script. 21 files were affected in total.	4329212.cif
78252	2013-04-01	cif/ Adding structures of 4329212 via cif-deposit CGI script.	4329212.cif