Crystallography Open Database

Information card for entry 4330888

Preview

Coordinates	4330888.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H68 Cl Ge N4 O Rh
Calculated formula	C42 H68 Cl Ge N4 O Rh
Title of publication	Bis(amidinato)germylenerhodium Complexes: Synthesis, Structure, and Density Functional Theory Calculations
Authors of publication	Dimitri Matioszek; Nathalie Saffon; Jean-Marc Sotiropoulos; Karinne Miqueu; Annie Castel; Jean Escudié
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	11716 - 11721
a	11.7561 ± 0.0005 Å
b	13.3498 ± 0.0006 Å
c	13.6919 ± 0.0006 Å
α	87.584 ± 0.002°
β	86.103 ± 0.002°
γ	87.405 ± 0.002°
Cell volume	2140.01 ± 0.16 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0307
Residual factor for significantly intense reflections	0.0261
Weighted residual factors for significantly intense reflections	0.068
Weighted residual factors for all reflections included in the refinement	0.0709
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179411 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/08.	4330888.cif
80347	2013-04-07	cif/ Adding structures of 4330888 via cif-deposit CGI script.	4330888.cif