Crystallography Open Database

Information card for entry 4330966

Preview

Coordinates	4330966.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H108 Ge2 N12 O88 Sb4 W18
Calculated formula	C24 H20 Ge2 O84 Sb4 W18
Title of publication	Synthesis and Biological Activity of Organoantimony(III)-Containing Heteropolytungstates
Authors of publication	Maria Barsukova-Stuckart; Luis F. Piedra-Garza; Bimersha Gautam; Gabriela Alfaro-Espinoza; Natalya V. Izarova; Abhishek Banerjee; Bassem S. Bassil; Matthias S. Ullrich; Hans J. Breunig; Cristian Silvestru; Ulrich Kortz
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	12015 - 12022
a	13.8872 ± 0.001 Å
b	17.9325 ± 0.0014 Å
c	20.7047 ± 0.0014 Å
α	74.469 ± 0.003°
β	77.786 ± 0.003°
γ	88.189 ± 0.003°
Cell volume	4853.7 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1116
Residual factor for significantly intense reflections	0.0549
Weighted residual factors for significantly intense reflections	0.1284
Weighted residual factors for all reflections included in the refinement	0.1667
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179412 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/09.	4330966.cif
80426	2013-04-07	cif/ Adding structures of 4330966 via cif-deposit CGI script.	4330966.cif