Crystallography Open Database

Information card for entry 4331514

Preview

Coordinates	4331514.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H35 Ge4 O6 Rh3
Calculated formula	C48 H35 Ge4 O6 Rh3
SMILES	[Rh]1234([Rh]56([Rh]1([Ge]5(c1ccccc1)c1ccccc1)([Ge]3(c1ccccc1)c1ccccc1)([Ge]46c1ccccc1)(C#[O])C#[O])([Ge]2(c1ccccc1)c1ccccc1)(C#[O])C#[O])(C#[O])C#[O]
Title of publication	Rhodium Cluster Complexes Containing Bridging Phenylgermanium Ligands
Authors of publication	Adams, Richard D.; Smith, Jack L.
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Journal issue	12
Pages of publication	4276 - 4281
a	11.5977 ± 0.001 Å
b	12.9543 ± 0.0011 Å
c	17.4276 ± 0.0015 Å
α	98.147 ± 0.002°
β	94.135 ± 0.002°
γ	113.94 ± 0.002°
Cell volume	2344.5 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0707
Residual factor for significantly intense reflections	0.0545
Weighted residual factors for significantly intense reflections	0.1322
Weighted residual factors for all reflections included in the refinement	0.1446
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179418 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/15.	4331514.cif
97673	2014-01-29	cif/ Adding structures of 4331514 via cif-deposit CGI script.	4331514.cif