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Information card for entry 4331540
Preview
| Coordinates | 4331540.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C156 H158 F48 N38 O6 P8 Pd8 |
|---|---|
| Calculated formula | C156 H158 F48 N38 O6 P8 Pd8 |
| Title of publication | Solution self-assembly, spontaneous deprotonation, and crystal structures of bipyrazolate-bridged metallomacrocycles with dimetal centers. |
| Authors of publication | Yu, Shu-Yan; Huang, Hai-Ping; Li, Sheng-Hui; Jiao, Qing; Li, Yi-Zhi; Wu, Biao; Sei, Yoshihisa; Yamaguchi, Kentaro; Pan, Yuan-Jiang; Ma, Hong-Wei |
| Journal of publication | Inorganic chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Journal issue | 25 |
| Pages of publication | 9471 - 9488 |
| a | 12.454 ± 0.002 Å |
| b | 22.437 ± 0.004 Å |
| c | 27.684 ± 0.005 Å |
| α | 77.492 ± 0.004° |
| β | 78.918 ± 0.004° |
| γ | 82.733 ± 0.004° |
| Cell volume | 7382 ± 2 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0958 |
| Residual factor for significantly intense reflections | 0.0639 |
| Weighted residual factors for significantly intense reflections | 0.1575 |
| Weighted residual factors for all reflections included in the refinement | 0.166 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179418 (current) | 2016-03-23 | cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/15. |
4331540.cif |
| 120066 | 2014-07-11 | cif/ Updating files of 4331538, 4331539, 4331540, 4331541, 4331542, 4331543 Original log message: Adding full bibliography for 4331538--4331543.cif. |
4331540.cif |
| 97693 | 2014-01-29 | cif/ Adding structures of 4331538, 4331539, 4331540, 4331541, 4331542, 4331543 via cif-deposit CGI script. |
4331540.cif |
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Users of the data should acknowledge the original authors of the
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