Crystallography Open Database

Information card for entry 4331630

Preview

Coordinates	4331630.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C88 H63 Mo N6 O4 P4
Calculated formula	C88 H63 Mo N6 O4 P4
Title of publication	Preparation, Characterization, and Reactivity of Dinitrogen Molybdenum Complexes with Bis(diphenylphosphino)amine Derivative Ligands that Form a Unique 4-Membered P-N-P Chelate Ring
Authors of publication	Takahiko Ogawa; Yuji Kajita; Yuko Wasada-Tsutsui; Hiroaki Wasada; Hideki Masuda
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	182 - 195
a	11.273 ± 0.004 Å
b	18.535 ± 0.006 Å
c	20.253 ± 0.007 Å
α	95.201 ± 0.005°
β	94.064 ± 0.004°
γ	102.522 ± 0.005°
Cell volume	4096 ± 2 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.0737
Weighted residual factors for all reflections included in the refinement	0.2261
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179419 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/16.	4331630.cif
97758	2014-01-29	cif/ Adding structures of 4331630 via cif-deposit CGI script.	4331630.cif