Crystallography Open Database

Information card for entry 4331636

Preview

Coordinates	4331636.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C67 H58 Mo N6 O P4
Calculated formula	C67 H58 Mo N6 O P4
Title of publication	Preparation, Characterization, and Reactivity of Dinitrogen Molybdenum Complexes with Bis(diphenylphosphino)amine Derivative Ligands that Form a Unique 4-Membered P-N-P Chelate Ring
Authors of publication	Takahiko Ogawa; Yuji Kajita; Yuko Wasada-Tsutsui; Hiroaki Wasada; Hideki Masuda
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	182 - 195
a	14.7122 ± 0.0006 Å
b	23.2371 ± 0.0006 Å
c	18.0126 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	6157.9 ± 0.4 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for significantly intense reflections	0.0392
Weighted residual factors for all reflections included in the refinement	0.1152
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179419 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/16.	4331636.cif
97764	2014-01-29	cif/ Adding structures of 4331636 via cif-deposit CGI script.	4331636.cif