Crystallography Open Database

Information card for entry 4331828

Preview

Coordinates	4331828.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H48 Ag2 N14 O7
Calculated formula	C36 H48 Ag2 N14 O6.5
Title of publication	Different Nuclearity Silver(I) Complexes with Novel Tetracyano Pendant-Armed Hexaazamacrocyclic Ligands
Authors of publication	del Carmen Fernández-Fernández, María; Bastida, Rufina; Macías, Alejandro; Pérez-Lourido, Paulo; Valencia, Laura
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	5
Pages of publication	2266 - 2275
a	12.8512 ± 0.0015 Å
b	26.383 ± 0.003 Å
c	13.1437 ± 0.0016 Å
α	90°
β	94.859 ± 0.002°
γ	90°
Cell volume	4440.4 ± 0.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1099
Residual factor for significantly intense reflections	0.0504
Weighted residual factors for significantly intense reflections	0.1161
Weighted residual factors for all reflections included in the refinement	0.1314
Goodness-of-fit parameter for all reflections included in the refinement	0.893
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179421 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/18.	4331828.cif
97926	2014-01-29	cif/ Adding structures of 4331825, 4331826, 4331827, 4331828 via cif-deposit CGI script.	4331828.cif