Crystallography Open Database

Information card for entry 4331860

Preview

Coordinates	4331860.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H47 Cl4 Co4 N4 O9.5
Calculated formula	C30 H38 Cl4 Co4 N4 O9.5
Title of publication	Boxes, Helicates, and Coordination Polymers: A Structural and Magnetochemical Investigation of the Diverse Coordination Chemistry of Simple Pyridine-Alcohol Ligands
Authors of publication	Telfer, Shane G.; Kuroda, Reiko; Lefebvre, Julie; Leznoff, Daniel B.
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	12
Pages of publication	4592 - 4601
a	14.9668 ± 0.0017 Å
b	17.3572 ± 0.0019 Å
c	31.227 ± 0.004 Å
α	90°
β	102.65 ± 0.002°
γ	90°
Cell volume	7915.3 ± 1.6 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1332
Residual factor for significantly intense reflections	0.0711
Weighted residual factors for significantly intense reflections	0.1729
Weighted residual factors for all reflections included in the refinement	0.2006
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4331860.cif
97943	2014-01-29	cif/ Adding structures of 4331860, 4331861, 4331862, 4331863, 4331864 via cif-deposit CGI script.	4331860.cif