Crystallography Open Database

Information card for entry 4332405

Preview

Coordinates	4332405.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H36 Ge8 N4
Calculated formula	C12 H36 Ge8 N4
Title of publication	Synthesis and Characterization of Imidocubanes with Exocube GeIVand SnIVSubstituents: [M(μ3-NGeMe3)]4(M = Sn, Ge, Pb); [Sn(μ3-NSnMe3)]4
Authors of publication	Eichler, Jack F.; Just, Oliver; Rees, William S.
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	17
Pages of publication	6706 - 6712
a	11.2872 ± 0.001 Å
b	11.2872 ± 0.001 Å
c	11.2872 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	1438 ± 0.2 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	4
Space group number	217
Hermann-Mauguin space group symbol	I -4 3 m
Hall space group symbol	I -4 2 3
Residual factor for all reflections	0.0411
Residual factor for significantly intense reflections	0.0339
Weighted residual factors for significantly intense reflections	0.0757
Weighted residual factors for all reflections included in the refinement	0.078
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179427 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/24.	4332405.cif
98296	2014-01-29	cif/ Adding structures of 4332405 via cif-deposit CGI script.	4332405.cif