Crystallography Open Database

Information card for entry 4332683

Preview

Coordinates	4332683.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H32 K4 O46 Ru2 Si W10
Calculated formula	C12 K4 O45.7 Ru2 Si W10
Title of publication	Dilacunary Decatungstates Functionalized by Organometallic Ruthenium(II), [{Ru(C6H6)(H2O)}{Ru(C6H6)}(γ-XW10O36)]4-(X = Si, Ge)
Authors of publication	Bi, Li-Hua; Chubarova, Elena V.; Nsouli, Nadeen H.; Dickman, Michael H.; Kortz, Ulrich; Keita, Bineta; Nadjo, Louis
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	21
Pages of publication	8575 - 8583
a	13.6702 ± 0.0003 Å
b	16.2419 ± 0.0004 Å
c	12.1397 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	2695.38 ± 0.1 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	31
Hermann-Mauguin space group symbol	P m n 21
Hall space group symbol	P 2ac -2
Residual factor for all reflections	0.0788
Residual factor for significantly intense reflections	0.0571
Weighted residual factors for significantly intense reflections	0.1399
Weighted residual factors for all reflections included in the refinement	0.1564
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179429 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/26.	4332683.cif
98478	2014-01-30	cif/ Adding structures of 4332683, 4332684 via cif-deposit CGI script.	4332683.cif