Crystallography Open Database

Information card for entry 4333863

Preview

Coordinates	4333863.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C79.75 H58.75 Cl0.75 F10 P5 Pt3
Calculated formula	C79.75 H58.75 Cl0.75 F10 P5 Pt3
Title of publication	Synthesis and Reactivity of the Unsaturated Trinuclear Phosphanido Complex [(C6F5)2Pt(μ-PPh2)2Pt(μ-PPh2)2Pt(PPh3)]
Authors of publication	Juan Forniés; Consuelo Fortuño; Susana Ibáñez; Antonio Martín; Piero Mastrorilli; Vito Gallo; Athanassios Tsipis
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	1942 - 1953
a	16.0336 ± 0.0011 Å
b	19.2639 ± 0.0013 Å
c	23.2512 ± 0.0016 Å
α	90°
β	101.592 ± 0.001°
γ	90°
Cell volume	7035.1 ± 0.8 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0529
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.0568
Weighted residual factors for all reflections included in the refinement	0.0588
Goodness-of-fit parameter for all reflections included in the refinement	0.991
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179441 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/38.	4333863.cif
99671	2014-02-03	cif/ Adding structures of 4333863 via cif-deposit CGI script.	4333863.cif