Crystallography Open Database

Information card for entry 4333983

Preview

Coordinates	4333983.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C83 H100 Cl3 Ho4 N10 O23
Calculated formula	C83 H88 Cl3 Ho4 N10 O23
Title of publication	New Structural Form of a Tetranuclear Lanthanide Hydroxo Cluster: Dy4 Analogue Display Slow Magnetic Relaxation
Authors of publication	Ananda Kumar Jami; Viswanathan Baskar; E. Carolina Sañudo
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	2432 - 2438
a	13.9722 ± 0.0017 Å
b	14.9105 ± 0.0018 Å
c	22.133 ± 0.003 Å
α	73.726 ± 0.002°
β	76.97 ± 0.002°
γ	85.834 ± 0.002°
Cell volume	4312.1 ± 0.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0416
Residual factor for significantly intense reflections	0.0373
Weighted residual factors for significantly intense reflections	0.0832
Weighted residual factors for all reflections included in the refinement	0.0852
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179442 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/39.	4333983.cif
99792	2014-02-03	cif/ Adding structures of 4333983 via cif-deposit CGI script.	4333983.cif