Crystallography Open Database

Information card for entry 4333987

Preview

Coordinates	4333987.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H32 Co P Si2
Calculated formula	C20 H32 Co P Si2
Title of publication	Synthesis of a Bis(indenyl) Co(I) Anion: A Reactive Source of a 14 Electron Indenyl Co(I) Equivalent
Authors of publication	Fernando Hung-Low; Christopher A. Bradley
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	2446 - 2457
a	17.216 ± 0.003 Å
b	17.694 ± 0.003 Å
c	7.5668 ± 0.0015 Å
α	90°
β	90°
γ	90°
Cell volume	2305 ± 0.7 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0425
Residual factor for significantly intense reflections	0.0352
Weighted residual factors for significantly intense reflections	0.1005
Weighted residual factors for all reflections included in the refinement	0.1063
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179442 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/39.	4333987.cif
99796	2014-02-03	cif/ Adding structures of 4333987 via cif-deposit CGI script.	4333987.cif