Crystallography Open Database

Information card for entry 4334182

Preview

Coordinates	4334182.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H36 Ag Al F28 O9 Si6
Calculated formula	C24 H36 Ag Al F28 O9 Si6
Title of publication	Reactions of a Cyclodimethylsiloxane (Me2SiO)6 with Silver Salts of Weakly Coordinating Anions; Crystal Structures of [Ag(Me2SiO)6][Al] ([Al] = [FAl{OC(CF3)3}3], [Al{OC(CF3)3}4]) and Their Comparison with [Ag(18-Crown-6)]2[SbF6]2
Authors of publication	T. Stanley Cameron; Andreas Decken; Ingo Krossing; Jack Passmore; J. Mikko Rautiainen; Xinping Wang; Xiaoqing Zeng
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	3113 - 3126
a	12.99 ± 0.003 Å
b	21.368 ± 0.004 Å
c	18.082 ± 0.004 Å
α	90°
β	93.199 ± 0.004°
γ	90°
Cell volume	5011.2 ± 1.9 Å³
Cell temperature	173 ± 1 K
Ambient diffraction temperature	173 ± 1 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1306
Residual factor for significantly intense reflections	0.0686
Weighted residual factors for significantly intense reflections	0.1988
Weighted residual factors for all reflections included in the refinement	0.2163
Goodness-of-fit parameter for all reflections included in the refinement	1.13
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179444 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/41.	4334182.cif
99996	2014-02-04	cif/ Adding structures of 4334182 via cif-deposit CGI script.	4334182.cif