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Information card for entry 4334544
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| Coordinates | 4334544.cif |
|---|---|
| Structure factors | 4334544.hkl |
| Original paper (by DOI) | HTML |
| Formula | C49 H77 Br2 N2 Si |
|---|---|
| Calculated formula | C49 H77 Br2 N2 Si |
| Title of publication | Easy Access to Silicon(0) and Silicon(II) Compounds |
| Authors of publication | Kartik Chandra Mondal; Prinson P. Samuel; Mykyta Tretiakov; Amit Pratap Singh; Herbert W. Roesky; A. Claudia Stückl; Benedikt Niepötter; Elena Carl; Hilke Wolf; Regine Herbst-Irmer; Dietmar Stalke |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2013 |
| Journal volume | 52 |
| Pages of publication | 4736 - 4743 |
| a | 13.176 ± 0.003 Å |
| b | 16.8 ± 0.002 Å |
| c | 20.681 ± 0.002 Å |
| α | 90° |
| β | 93.57 ± 0.02° |
| γ | 90° |
| Cell volume | 4569 ± 1.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.047 |
| Residual factor for significantly intense reflections | 0.0304 |
| Weighted residual factors for significantly intense reflections | 0.0604 |
| Weighted residual factors for all reflections included in the refinement | 0.0652 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.01 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181932 (current) | 2016-04-07 | hkl/4/ (antanas@echidna.ibt.lt) Adding svn headers to multiple entries in subrange 4/33. |
4334544.cif 4334544.hkl |
| 180700 | 2016-04-02 | cod/ (antanas@echidna.ibt.lt) Setting the 'svn:keywords' property for all '*.hkl' files that were previously unaffected by this property. |
4334544.cif 4334544.hkl |
| 179448 | 2016-03-23 | cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/45. |
4334544.cif 4334544.hkl |
| 103164 | 2014-02-25 | hkl/4 Adding Fobs files for entries coming from J. Org. Chem. and Inorg. Chem. 2013 |
4334544.cif 4334544.hkl |
| 100372 | 2014-02-04 | cif/ Adding structures of 4334544 via cif-deposit CGI script. |
4334544.cif |
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Users of the data should acknowledge the original authors of the
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