Crystallography Open Database

Information card for entry 4334620

Preview

Coordinates	4334620.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	bis(2,2'-Bipyridyl)-tris(μ2-1,3-bis(4,4,4-Trifluoro-3-oxido- 1-(oxo)but-2-en-1-yl)phenyl)-di-europium(iii) dichloromethane solvate
Formula	C64 H38 Cl4 Eu2 F18 N4 O12
Calculated formula	C64 H38 Cl4 Eu2 F18 N4 O12
Title of publication	Crystal Structure and Highly Luminescent Properties Studies of Bis-β-diketonate Lanthanide Complexes
Authors of publication	Jing Shi; Yanjun Hou; Wenyi Chu; Xiaohong Shi; Huiquan Gu; Bilin Wang; Zhizhong Sun
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	5013 - 5022
a	12.3302 ± 0.0004 Å
b	15.1832 ± 0.0005 Å
c	19.6047 ± 0.0007 Å
α	96.92°
β	103.56°
γ	91.55°
Cell volume	3536.1 ± 0.2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0381
Residual factor for significantly intense reflections	0.0329
Weighted residual factors for significantly intense reflections	0.0876
Weighted residual factors for all reflections included in the refinement	0.0919
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179449 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/46.	4334620.cif
100490	2014-02-06	cif/ Adding structures of 4334620 via cif-deposit CGI script.	4334620.cif