Crystallography Open Database

Information card for entry 4334677

Preview

Coordinates	4334677.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Trimethylsilylisonitrile/trimethylsilylnitrile galliumtrichloride adduct
Formula	C4 H9 Cl3 Ga N Si
Calculated formula	C4 H9 Cl3 Ga N Si
Title of publication	On the Synthesis and Reactivity of Highly Labile Pseudohalogen Phosphenium Ions
Authors of publication	Christian Hering; Axel Schulz; Alexander Villinger
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	5214 - 5225
a	9.935 ± 0.0005 Å
b	9.935 ± 0.0005 Å
c	9.5741 ± 0.0008 Å
α	90°
β	90°
γ	120°
Cell volume	818.4 ± 0.09 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	146
Hermann-Mauguin space group symbol	R 3 :H
Hall space group symbol	R 3
Residual factor for all reflections	0.0215
Residual factor for significantly intense reflections	0.0195
Weighted residual factors for significantly intense reflections	0.035
Weighted residual factors for all reflections included in the refinement	0.0353
Goodness-of-fit parameter for all reflections included in the refinement	0.943
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179449 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/46.	4334677.cif
100547	2014-02-06	cif/ Adding structures of 4334677 via cif-deposit CGI script.	4334677.cif