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Information card for entry 4334978
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Coordinates | 4334978.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H44 O Os P2 |
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Calculated formula | C27 H44 O Os P2 |
Title of publication | POP-Pincer Osmium-Polyhydrides: Head-to-Head (Z)-Dimerization of Terminal Alkynes |
Authors of publication | Joaquín Alós; Tamara Bolaño; Miguel A. Esteruelas; Montserrat Oliván; Enrique Oñate; Marta Valencia |
Journal of publication | Inorganic Chemistry |
Year of publication | 2013 |
Journal volume | 52 |
Pages of publication | 6199 - 6213 |
a | 22.5833 ± 0.0014 Å |
b | 21.4733 ± 0.0014 Å |
c | 45.431 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 22031 ± 2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.092 |
Residual factor for significantly intense reflections | 0.0377 |
Weighted residual factors for significantly intense reflections | 0.0611 |
Weighted residual factors for all reflections included in the refinement | 0.075 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
179452 (current) | 2016-03-23 | cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/49. |
4334978.cif |
100864 | 2014-02-07 | cif/ Adding structures of 4334978 via cif-deposit CGI script. |
4334978.cif |
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Users of the data should acknowledge the original authors of the
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