Crystallography Open Database

Information card for entry 4334989

Preview

Coordinates	4334989.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H18 Co F12 N4
Calculated formula	C29 H17.5 Co F12 N4
Title of publication	Correction to 2,2'-Pyridylpyrrolide Ligand Redistribution Following Reduction
Authors of publication	Keith Searles; Atanu K. Das; René W. Buell; Maren Pink; Chun-Hsing Chen; Kuntal Pal; David Gene Morgan; Daniel J. Mindiola; Kenneth G. Caulton
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	6231 - 6231
a	12.8161 ± 0.0019 Å
b	27.136 ± 0.004 Å
c	35.312 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	12281 ± 3 Å³
Cell temperature	250 ± 2 K
Ambient diffraction temperature	250 ± 2 K
Number of distinct elements	5
Space group number	70
Hermann-Mauguin space group symbol	F d d d :2
Hall space group symbol	-F 2uv 2vw
Residual factor for all reflections	0.0669
Residual factor for significantly intense reflections	0.0488
Weighted residual factors for significantly intense reflections	0.1363
Weighted residual factors for all reflections included in the refinement	0.1525
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179452 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/49.	4334989.cif
100875	2014-02-07	cif/ Adding structures of 4334989 via cif-deposit CGI script.	4334989.cif