Crystallography Open Database

Information card for entry 4335122

Preview

Coordinates	4335122.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	B4 H2 O13 Pb6
Calculated formula	B4 O13 Pb6
Title of publication	Facile Assembly of an Unusual Lead Borate with Different Cluster Building Units via a Hydrothermal Process
Authors of publication	Han-Rui Tian; Wen-Hua Wang; Yan-E Gao; Ting-Ting Deng; Jia-Ying Wang; Yun-Long Feng; Jian-Wen Cheng
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	6242 - 6244
a	13.3931 ± 0.0015 Å
b	13.0149 ± 0.0016 Å
c	7.8019 ± 0.001 Å
α	90°
β	90°
γ	90°
Cell volume	1359.9 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0722
Residual factor for significantly intense reflections	0.0679
Weighted residual factors for significantly intense reflections	0.1613
Weighted residual factors for all reflections included in the refinement	0.1657
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179454 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/51.	4335122.cif
101027	2014-02-10	cif/ Adding structures of 4335122 via cif-deposit CGI script.	4335122.cif