Crystallography Open Database

Information card for entry 4335126

Preview

Coordinates	4335126.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20.5 H43 B10 Cl Rh2
Calculated formula	C20.5 H42 B10 Cl Rh2
Title of publication	Supraicosahedral Polyhedra in Metallaboranes: Synthesis and Structural Characterization of 12-, 15-, and 16-Vertex Rhodaboranes
Authors of publication	Dipak Kumar Roy; Bijan Mondal; Pritam Shankhari; R. S. Anju; K. Geetharani; Shaikh M. Mobin; Sundargopal Ghosh
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	6705 - 6712
a	33.3146 ± 0.0015 Å
b	10.6577 ± 0.0004 Å
c	16.7985 ± 0.0007 Å
α	90°
β	111.424 ± 0.002°
γ	90°
Cell volume	5552.3 ± 0.4 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0865
Residual factor for significantly intense reflections	0.0475
Weighted residual factors for significantly intense reflections	0.1036
Weighted residual factors for all reflections included in the refinement	0.1214
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4335126.cif
101031	2014-02-10	cif/ Adding structures of 4335126 via cif-deposit CGI script.	4335126.cif