Crystallography Open Database

Information card for entry 4335207

Preview

Coordinates	4335207.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C78.5 H60.5 N8.5 O4 U
Calculated formula	C78.5 H60.5 N8.5 O4 U
Title of publication	Synthesis of Electron-Rich Uranium(IV) Complexes Supported by Tridentate Schiff Base Ligands and Their Multi-Electron Redox Chemistry
Authors of publication	Clément Camp; Julie Andrez; Jacques Pécaut; Marinella Mazzanti
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7078 - 7086
a	45.625 ± 0.002 Å
b	15.8387 ± 0.0009 Å
c	18.5959 ± 0.0013 Å
α	90°
β	110.506 ± 0.005°
γ	90°
Cell volume	12586.7 ± 1.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1181
Residual factor for significantly intense reflections	0.0623
Weighted residual factors for significantly intense reflections	0.1318
Weighted residual factors for all reflections included in the refinement	0.1654
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4335207.cif
101115	2014-02-10	cif/ Adding structures of 4335207 via cif-deposit CGI script.	4335207.cif