Crystallography Open Database

Information card for entry 4335252

Preview

Coordinates	4335252.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	F2 Na9 O20 Si4 U3
Calculated formula	F2 Na9 O20 Si4 U3
Title of publication	High-Temperature, High-Pressure Hydrothermal Synthesis and Characterization of a Salt-Inclusion Mixed-Valence Uranium(V,VI) Silicate: [Na9F2][(UVO2)(UVIO2)2(Si2O7)2]
Authors of publication	Yu-Chih Chang; Wen-Jung Chang; Sophie Boudin; Kwang-Hwa Lii
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7230 - 7235
a	5.7889 ± 0.0012 Å
b	7.4227 ± 0.0015 Å
c	12.092 ± 0.002 Å
α	90.75 ± 0.03°
β	96.09 ± 0.03°
γ	90.9 ± 0.03°
Cell volume	516.53 ± 0.17 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0259
Residual factor for significantly intense reflections	0.0241
Weighted residual factors for significantly intense reflections	0.0602
Weighted residual factors for all reflections included in the refinement	0.0612
Goodness-of-fit parameter for all reflections included in the refinement	1.11
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179455 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/52.	4335252.cif
101161	2014-02-10	cif/ Adding structures of 4335252 via cif-deposit CGI script.	4335252.cif