Crystallography Open Database

Information card for entry 4335254

Preview

Coordinates	4335254.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H36 Ge N8
Calculated formula	C27 H36 Ge N8
Title of publication	Synthesis and Structure of Base-Stabilized Germanium(II) Diazide IPrGe(N3)2
Authors of publication	Benjamin Lyhs; Dieter Bläser; Christoph Wölper; Stephan Schulz; Rebekka Haack; Georg Jansen
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7236 - 7241
a	16.5337 ± 0.0003 Å
b	9.4188 ± 0.0002 Å
c	17.794 ± 0.0004 Å
α	90°
β	90.631 ± 0.001°
γ	90°
Cell volume	2770.85 ± 0.1 Å³
Cell temperature	100 ± 1 K
Ambient diffraction temperature	100 ± 1 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0551
Residual factor for significantly intense reflections	0.0412
Weighted residual factors for significantly intense reflections	0.1095
Weighted residual factors for all reflections included in the refinement	0.1168
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179455 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/52.	4335254.cif
101163	2014-02-10	cif/ Adding structures of 4335254 via cif-deposit CGI script.	4335254.cif