Crystallography Open Database

Information card for entry 4335292

Preview

Coordinates	4335292.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C111.84 H178.02 Cl4 N4 O4 U2
Calculated formula	C111.84 H178.016 Cl4 N4 O4 U2
Title of publication	"Oxidative Addition" of Halogens to Uranium(IV) Bis(amidophenolate) Complexes
Authors of publication	Ellen M. Matson; Stacey R. Opperwall; Phillip E. Fanwick; Suzanne C. Bart
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7295 - 7304
a	33.2139 ± 0.0013 Å
b	15.5613 ± 0.0008 Å
c	23.525 ± 0.0011 Å
α	90°
β	96.585 ± 0.001°
γ	90°
Cell volume	12078.7 ± 1 Å³
Cell temperature	150 ± 0.02 K
Ambient diffraction temperature	150 ± 0.02 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.084
Residual factor for significantly intense reflections	0.058
Weighted residual factors for significantly intense reflections	0.115
Weighted residual factors for all reflections included in the refinement	0.124
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MO-Kα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179455 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/52.	4335292.cif
101201	2014-02-10	cif/ Adding structures of 4335292 via cif-deposit CGI script.	4335292.cif