Crystallography Open Database

Information card for entry 4335360

Preview

Coordinates	4335360.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H86 N6 O15 P2 Pd6
Calculated formula	C48 H84 N6 O15 P2 Pd6
Title of publication	Facile Formation of Stable Tris(imido)phosphate Trianions as Their Tri- and Hexanuclear Pd(II) Complexes in Protic Solvents
Authors of publication	Arvind K. Gupta; S. Arun Dixith Reddy; Ramamoorthy Boomishankar
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7608 - 7614
a	15.31 ± 0.002 Å
b	21.694 ± 0.002 Å
c	19.245 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	6391.9 ± 1.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	20
Hermann-Mauguin space group symbol	C 2 2 21
Hall space group symbol	C 2c 2
Residual factor for all reflections	0.1158
Residual factor for significantly intense reflections	0.06
Weighted residual factors for significantly intense reflections	0.1135
Weighted residual factors for all reflections included in the refinement	0.1338
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179456 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/53.	4335360.cif
101286	2014-02-11	cif/ Adding structures of 4335360 via cif-deposit CGI script.	4335360.cif