Crystallography Open Database

Information card for entry 4335363

Preview

Coordinates	4335363.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H68 N6 O14 P2 Pd6 S2
Calculated formula	C30 H68 N6 O14 P2 Pd6 S2
Title of publication	Facile Formation of Stable Tris(imido)phosphate Trianions as Their Tri- and Hexanuclear Pd(II) Complexes in Protic Solvents
Authors of publication	Arvind K. Gupta; S. Arun Dixith Reddy; Ramamoorthy Boomishankar
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7608 - 7614
a	24.812 ± 0.003 Å
b	9.7381 ± 0.0014 Å
c	23.628 ± 0.003 Å
α	90°
β	120.349 ± 0.002°
γ	90°
Cell volume	4926.7 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0541
Residual factor for significantly intense reflections	0.0373
Weighted residual factors for significantly intense reflections	0.081
Weighted residual factors for all reflections included in the refinement	0.0887
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179456 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/53.	4335363.cif
101290	2014-02-11	cif/ Adding structures of 4335363 via cif-deposit CGI script.	4335363.cif