Crystallography Open Database

Information card for entry 4335428

Preview

Coordinates	4335428.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	DMF@[Ag4(tppepb)4]I4
Formula	C276 H208.48 Ag4 I4 N4 O4 P12
Calculated formula	C276 H208.48 Ag4 I4 N4 O4 P12
Title of publication	Self-Assembled Supramolecular Clusters Based on Phosphines and Coinage Metals: Tetrahedra, Helicates, and Mesocates
Authors of publication	Sang Ho Lim; Seth M. Cohen
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7862 - 7872
a	69.8512 ± 0.0018 Å
b	19.7868 ± 0.0005 Å
c	38.2622 ± 0.0011 Å
α	90°
β	92.882 ± 0.002°
γ	90°
Cell volume	52817 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0907
Residual factor for significantly intense reflections	0.0814
Weighted residual factors for significantly intense reflections	0.2373
Weighted residual factors for all reflections included in the refinement	0.2485
Goodness-of-fit parameter for all reflections included in the refinement	1.09
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179457 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/54.	4335428.cif
101357	2014-02-13	cif/ Adding structures of 4335428 via cif-deposit CGI script.	4335428.cif