Crystallography Open Database

Information card for entry 4337010

Preview

Coordinates	4337010.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C130 H213 Ga6 N14 Ni8
Calculated formula	C130 H213 Ga6 N14 Ni8
Title of publication	Clusters [Ma(GaCp*)b(CNR)c] (M = Ni, Pd, Pt): Synthesis, Structure, and Ga/Zn Exchange Reactions
Authors of publication	Mariusz Molon; Katharina Dilchert; Christian Gemel; Rüdiger W. Seidel; Julian Schaumann; Roland A. Fischer
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	14275 - 14283
a	14.9307 ± 0.0004 Å
b	22.7367 ± 0.0006 Å
c	24.1929 ± 0.0006 Å
α	73.638 ± 0.002°
β	88.638 ± 0.002°
γ	71.327 ± 0.002°
Cell volume	7445.5 ± 0.4 Å³
Cell temperature	105 ± 2 K
Ambient diffraction temperature	105 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0775
Residual factor for significantly intense reflections	0.0485
Weighted residual factors for significantly intense reflections	0.1149
Weighted residual factors for all reflections included in the refinement	0.1272
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179473 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/70.	4337010.cif
103076	2014-02-25	cif/ Adding structures of 4337010 via cif-deposit CGI script.	4337010.cif