Crystallography Open Database

Information card for entry 4337407

Preview

Coordinates	4337407.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H81 N2 O3 Si2 Yb
Calculated formula	C46 H81 N2 O3 Si2 Yb
Title of publication	Divalent heteroleptic ytterbium complexes - effective catalysts for intermolecular styrene hydrophosphination and hydroamination.
Authors of publication	Basalov, Ivan V.; Roşca, Sorin Claudiu; Lyubov, Dmitry M.; Selikhov, Alexander N.; Fukin, Georgy K.; Sarazin, Yann; Carpentier, Jean-François; Trifonov, Alexander A.
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	3
Pages of publication	1654 - 1661
a	18.6631 ± 0.0014 Å
b	24.0308 ± 0.0018 Å
c	10.9921 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	4929.8 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0733
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.0722
Weighted residual factors for all reflections included in the refinement	0.0787
Goodness-of-fit parameter for all reflections included in the refinement	0.978
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179477 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/74.	4337407.cif
106344	2014-03-15	cif/ Adding structures of 4337407 via cif-deposit CGI script.	4337407.cif