Crystallography Open Database

Information card for entry 4337430

Preview

Coordinates	4337430.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39.5 H56.5 Cl N4 O2.5 Yb
Calculated formula	C39.5 H56.5 Cl N4 O2.5 Yb
Title of publication	Reversible Switching of Coordination Mode of ansa bis(Amidinate) Ligand in Ytterbium Complexes Driven by Oxidation State of the Metal Atom.
Authors of publication	Tolpygin, Aleksei O.; Cherkasov, Anton V.; Fukin, Georgii K.; Trifonov, Alexander A.
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	3
Pages of publication	1537 - 1543
a	12.3731 ± 0.0007 Å
b	15.9925 ± 0.0009 Å
c	19.7268 ± 0.0011 Å
α	86.857 ± 0.001°
β	78.881 ± 0.001°
γ	82.954 ± 0.001°
Cell volume	3799.3 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0644
Residual factor for significantly intense reflections	0.0374
Weighted residual factors for significantly intense reflections	0.0805
Weighted residual factors for all reflections included in the refinement	0.0873
Goodness-of-fit parameter for all reflections included in the refinement	0.968
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4337430.cif
106369	2014-03-15	cif/ Adding structures of 4337429, 4337430, 4337431 via cif-deposit CGI script.	4337430.cif