Crystallography Open Database

Information card for entry 4337474

Preview

Coordinates	4337474.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H38 Cl Cu Ge I N5
Calculated formula	C30 H38 Cl Cu Ge I N5
SMILES	I[Cu]([Ge]1([N](CC(C)C)=C2C=CC=CC=C2N1CC(C)C)Cl)([n]1ccccc1)[n]1ccccc1.c1cnccc1
Title of publication	Aminotroponiminato(chloro)germylene stabilized copper(I) iodide complexes: synthesis and structure.
Authors of publication	Yadav, Dhirendra; Siwatch, Rahul Kumar; Sinhababu, Soumen; Nagendran, Selvarajan
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	1
Pages of publication	600 - 606
a	19.985 ± 0.003 Å
b	10.2202 ± 0.0017 Å
c	32.465 ± 0.006 Å
α	90°
β	90°
γ	90°
Cell volume	6631 ± 1.9 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	7
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0972
Residual factor for significantly intense reflections	0.0799
Weighted residual factors for significantly intense reflections	0.1615
Weighted residual factors for all reflections included in the refinement	0.1687
Goodness-of-fit parameter for all reflections included in the refinement	1.304
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179477 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/74.	4337474.cif
106398	2014-03-15	cif/ Adding structures of 4337473, 4337474, 4337475 via cif-deposit CGI script.	4337474.cif