Crystallography Open Database

Information card for entry 4337565

Preview

Coordinates	4337565.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tetra(N"-(2,2'-bipyridinetricarbony-rhenium(I))-N,N'-diphenyl- isonicotamidate)(acetonitrile)dirhodium(II) tetrakis(hexafluorophospate), acetonitrile disolvate
Formula	C130 H97 F24 N23 O12 P4 Re4 Rh2
Calculated formula	C130 H97 F24 N23 O12 P4 Re4 Rh2
Title of publication	Rhodium amidinate dimers as structural and functional hubs for multimetallic assemblies.
Authors of publication	Chartrand, Daniel; Hanan, Garry S.
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	1
Pages of publication	624 - 636
a	20.3501 ± 0.001 Å
b	26.4964 ± 0.0015 Å
c	26.964 ± 0.0019 Å
α	90°
β	90°
γ	90°
Cell volume	14539.1 ± 1.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.1374
Residual factor for significantly intense reflections	0.1087
Weighted residual factors for significantly intense reflections	0.2779
Weighted residual factors for all reflections included in the refinement	0.303
Goodness-of-fit parameter for all reflections included in the refinement	1.126
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179478 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/75.	4337565.cif
106466	2014-03-15	cif/ Adding structures of 4337565, 4337566 via cif-deposit CGI script.	4337565.cif