Crystallography Open Database

Information card for entry 4337877

Preview

Coordinates	4337877.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C76 H120 N32 Ni4 O16 W2
Calculated formula	C76 H120 N32 Ni4 O16 W2
Title of publication	1D to 3D Heterobimetallic Complexes Tuned by Cyanide Precursors: Synthesis, Crystal Structures, and Magnetic Properties.
Authors of publication	Zhang, Daopeng; Si, Weijiang; Wang, Ping; Chen, Xia; Jiang, Jianzhuang
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	7
Pages of publication	3494
a	26.2457 ± 0.0015 Å
b	13.9671 ± 0.0008 Å
c	29.8116 ± 0.0017 Å
α	90°
β	95.311 ± 0.001°
γ	90°
Cell volume	10881.3 ± 1.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.07
Residual factor for significantly intense reflections	0.0493
Weighted residual factors for significantly intense reflections	0.1363
Weighted residual factors for all reflections included in the refinement	0.1538
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179481 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/78.	4337877.cif
109911	2014-04-17	cif/ Updating files of 4337877, 4337878, 4337879, 4337880, 4337881 Original log message: Adding full bibliography for 4337877--4337881.cif.	4337877.cif
108458	2014-04-02	cif/ Adding structures of 4337877 via cif-deposit CGI script.	4337877.cif