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Information card for entry 4338308
Preview
| Coordinates | 4338308.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | B20 K26 O166 U40 |
|---|---|
| Calculated formula | B20 K26 O166 U40 |
| Title of publication | Further Evidence for the Stabilization of U(V) within a Tetraoxo Core. |
| Authors of publication | Stritzinger, Jared T.; Alekseev, Evgeny V.; Polinski, Matthew J.; Cross, Justin N.; Eaton, Teresa M.; Albrecht-Schmitt, Thomas E |
| Journal of publication | Inorganic chemistry |
| Year of publication | 2014 |
| Journal volume | 53 |
| Journal issue | 10 |
| Pages of publication | 5294 - 5299 |
| a | 13.3979 ± 0.0008 Å |
| b | 49.867 ± 0.003 Å |
| c | 6.9305 ± 0.0004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 4630.4 ± 0.5 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 55 |
| Hermann-Mauguin space group symbol | P b a m |
| Hall space group symbol | -P 2 2ab |
| Residual factor for all reflections | 0.0462 |
| Residual factor for significantly intense reflections | 0.0393 |
| Weighted residual factors for significantly intense reflections | 0.099 |
| Weighted residual factors for all reflections included in the refinement | 0.1006 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.885 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179486 (current) | 2016-03-23 | cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/83. |
4338308.cif |
| 130086 | 2015-01-23 | cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ | xargs -i sh -c 'cif_fix_values {} \ | cif_filter --add-cif-header {} \ | sponge {}' |
4338308.cif |
| 115710 | 2014-06-05 | cif/ Updating files of 4338307, 4338308 Original log message: Adding full bibliography for 4338307--4338308.cif. |
4338308.cif |
| 112637 | 2014-05-03 | cif/ Adding structures of 4338307, 4338308 via cif-deposit CGI script. |
4338308.cif |
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Users of the data should acknowledge the original authors of the
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