Crystallography Open Database

Information card for entry 4338861

Preview

Coordinates	4338861.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C183 H164 Au18 Cl9 P19
Calculated formula	C183 H164 Au18 Cl9 P19
Title of publication	Synthesis, characterization, and X-ray structure determination of [Au18(P)2(PPh)4(PHPh)(dppm)6]Cl3.
Authors of publication	Sevillano, Paloma; Fuhr, Olaf; Hampe, Oliver; Lebedkin, Sergej; Matern, Eberhard; Fenske, Dieter; Kappes, Manfred M.
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	18
Pages of publication	7294 - 7298
a	22.438 ± 0.005 Å
b	24.895 ± 0.005 Å
c	39.019 ± 0.008 Å
α	90°
β	90°
γ	90°
Cell volume	21796 ± 8 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	210 ± 2 K
Number of distinct elements	5
Space group number	20
Hermann-Mauguin space group symbol	C 2 2 21
Hall space group symbol	C 2c 2
Residual factor for all reflections	0.0558
Residual factor for significantly intense reflections	0.0534
Weighted residual factors for significantly intense reflections	0.1467
Weighted residual factors for all reflections included in the refinement	0.1491
Goodness-of-fit parameter for all reflections included in the refinement	1.128
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179491 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/88.	4338861.cif
116970	2014-06-14	cif/ Adding structures of 4338861 via cif-deposit CGI script.	4338861.cif